Nano zero-valent iron (nZVI), bimetallic Nano zero-valent iron-copper (Fe 0- Cu), and fava bean activated carbon-supported with bimetallic Nano zero-valent iron-copper (AC-F e 0-Cu) were prepared and characterized by DLS, FT-IR, XRD, and SEM. The influence of the synthesized adsorbents on the adsorption and removal of soluble anionic methyl orange (M.O) dye was investigated using UV-V spectroscopy